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Capillary Electrophoresis Methods for Pharmaceutical Analysis

Capillary Electrophoresis Methods for Pharmaceutical Analysis
A Book

by Satinder Ahuja,Mohamedilias Jimidar

  • Publisher : Elsevier
  • Release : 2011-08-09
  • Pages : 546
  • ISBN : 0080559611
  • Language : En, Es, Fr & De
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Capillary electrophoresis (CE) is a powerful analytical technique that is widely used in research and development and in quality control of pharmaceuticals. Many reports of highly efficient separations and methods have been published over the past 15 years. CE offers several advantages over high-pressure or high-performance liquid chromatography (HPLC). These include simplicity, rapid analysis, automation, ruggedness, different mechanisms for selectivity, and low cost. Moreover, EC requires smaller sample size and yet offers higher efficiency and thus greater resolution power over HPLC. These characteristics are very attractive in research and development, even more so in pharmaceutical quality control (QC) and stability monitoring (SM) studies. This book will provide busy pharmaceutical scientists a complete yet concise reference guide for utilizing the versatility of CE in new drug development and quality control. - Provides current status and future developments in CE analysis of pharmaceuticals. - Explains how to develop and validate methods. - Includes major pharmaceutical applications including assays and impurity testing.

Capillary Electrophoresis Methods for Pharmaceutical Analysis

Capillary Electrophoresis Methods for Pharmaceutical Analysis
A Book

by George Lunn

  • Publisher : Wiley-Interscience
  • Release : 2000-02-21
  • Pages : 1544
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Capillary Electrophoresis Techniques for Pharmaceutical Analysis at your fingertips-A complete, up-to-date library. This invaluable database--also available on CD-ROM--gives you fast, easy access to the growing literature on capillary electrophoresis (CE). Nearly 3,000 abstracts from approximately 900 publications make up this comprehensive library, listing CE techniques for the analysis of more than 700 active pharmaceutical compounds. From acarbose to mephobarbital to zopiclone--a number of procedures are grouped together for each compound. Detailed, precise information lets you replicate methods without referring to original articles as well as customize methods for specific needs. Features include: * Methods for drugs in biological fluids such as blood or urine as well as for bulk and formulated drugs * Name and structure of each target compound as well as molecular weight and formula, CAS registry numbers, and Merck index number * Experimental conditions for each method, including sample preparation, analytical matrix, capillary/capillary instrument model, capillary temperature, interfering compounds, and more * Bibliography of reviews of capillary electrophoresis procedures The CD-ROM additionally combines the four-volume HPLC Methods for Pharmaceutical Analysis with thousands of methods listed for more than 1,300 compounds. This immensely useful reference will save you countless hours of online and library research.

Capillary Electrophoresis Methods For Pharmaceutical Analysis

Capillary Electrophoresis Methods For Pharmaceutical Analysis
A Book

by Ahuja

  • Publisher : Unknown Publisher
  • Release : 2009-01-01
  • Pages : 529
  • ISBN : 9788131219416
  • Language : En, Es, Fr & De
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Capillary Electrophoresis

Capillary Electrophoresis
Methods and Protocols

by Philippe Schmitt-Kopplin

  • Publisher : Springer Science & Business Media
  • Release : 2008-02-25
  • Pages : 814
  • ISBN : 1588295397
  • Language : En, Es, Fr & De
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This book presents a selection of current capillary electrophoresis methods used to separate representative types of molecules and particles and in combination with different detection techniques. It includes practical details which are hard to find elsewhere. The volume is intended for beginners in the field and provides an overview of the technique and a starting point for the exploration of the defined literature on different application topics.

Development of Capillary Electrophoresis Methods Coupled to Mass Spectrometry for Biomedical and Pharmaceutical Analysis

Development of Capillary Electrophoresis Methods Coupled to Mass Spectrometry for Biomedical and Pharmaceutical Analysis
A Book

by Anisa Elhamili

  • Publisher : Unknown Publisher
  • Release : 2011
  • Pages : 64
  • ISBN : 9789155479961
  • Language : En, Es, Fr & De
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Capillary Electrophoresis for Food Analysis

Capillary Electrophoresis for Food Analysis
Method Development

by Richard A. Frazier,H. E. Nursten,Jennifer M. Ames

  • Publisher : Royal Society of Chemistry
  • Release : 2000
  • Pages : 127
  • ISBN : 9780854044924
  • Language : En, Es, Fr & De
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Shows food analysts ways to use the capillary electrophoresis (CE) technique for the development of new separation methods specifically for food analysis. After describing CE theory and its modes of separation and detection, the authors (food chemistry, University of Reading) walk step by step through the method development process, detailing resolution, stability, and quantification goals. The handbook concentrates on the two most commonly encountered modes of CE--capillary zone electrophoresis and micellar electrokinetic chromatography. Case studies apply CE to the separation of niacin, green tea catechins, and artificial sweeteners and colors in soft drinks. Annotation copyrighted by Book News, Inc., Portland, OR

HPLC Methods for Pharmaceutical Analysis

HPLC Methods for Pharmaceutical Analysis
A Book

by George Lunn,Norman R. Schmuff

  • Publisher : Wiley-Interscience
  • Release : 1997
  • Pages : 1856
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Full text included in Knovel Library within the subject area of Chemistry and Chemical Engineering.

Encyclopedia of Analytical Science

Encyclopedia of Analytical Science
A Book

by Anonim

  • Publisher : Elsevier
  • Release : 2019-04-02
  • Pages : 5109
  • ISBN : 008101984X
  • Language : En, Es, Fr & De
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The third edition of the Encyclopedia of Analytical Science is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher

Pharmaceutical Analysis E-Book

Pharmaceutical Analysis E-Book
A Textbook for Pharmacy Students and Pharmaceutical Chemists

by David G. Watson

  • Publisher : Elsevier Health Sciences
  • Release : 2012-07-15
  • Pages : 406
  • ISBN : 0702051292
  • Language : En, Es, Fr & De
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An introductory text, written with the needs of the student in mind, which explains all the most important techniques used in the analysis of pharmaceuticals - a key procedure in ensuring the quality of drugs . The text is enhanced throughout with keypoints and self-assessment boxes, to aid student learning. Features Includes worked calculations to demonstrate mathematics in use for pharmaceutical analysis. Focuses on key points rather than a large number of facts to help readers really understand the field as well as pass exams. Includes self-assessment, focussing on simple arithmetical calculation results from analytical data. Additional section on basic calculations in pharmaceutical analysis More detail on the capillary electrophoresis of proteins A discussion of some of the new types of HPLC column and on solvent selectivity in HPLC Additional material inserted on the control of the quality of analytical methods, mass spectrometry and high pressure liquid chromatography Additional self-assessment exercises

Journal of Capillary Electrophoresis

Journal of Capillary Electrophoresis
A Book

by Anonim

  • Publisher : Unknown Publisher
  • Release : 2004
  • Pages : 329
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Chiral Capillary Electrophoresis in Current Pharmaceutical and Biomedical Analysis

Chiral Capillary Electrophoresis in Current Pharmaceutical and Biomedical Analysis
A Book

by Peter Mikuš

  • Publisher : BoD – Books on Demand
  • Release : 2012-08-29
  • Pages : 210
  • ISBN : 9535106570
  • Language : En, Es, Fr & De
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The scientific monograph by the author Peter Mikus entitled "Chiral Capillary Electrophoresis in Current Pharmaceutical and Biomedical Analysis" provides a comprehensive view on the advanced capillary electrophoresis techniques aimed to current chiral bioanalysis. The advances in the chiral electrophoresis analytical approaches are divided and theoretically described in three sections involving (i) advanced chiral separations for the optimization of chiral resolution (separation mechanisms; electrophoresis techniques in capillary and microchip format; electrophoretic modes such as ITP, CZE/EKC, CEC; chiral additives / pseudophases / phases), (ii) advanced sample preparation for the on-line preconcentration, sample clean-up and analyte derivatization (implementation of electrophoretic effects such as stacking; non-electrophoretic effects such as SPE, chromatography, dialysis; combinations of these effects; multidimensional CE systems; instrumental schemes), (iii) advanced combinations of detection and electrophoresis for the optimization in qualitative and quantitative evaluation (the most important universal as well as selective detection approaches such as absorption and fluorescence spectrophotometry, electrochemical detection, mass spectrometry vs. (i) and/or (ii)). Real analytical potential (benefits and limitations) of these advanced analytical approaches is emphasized by selected performance parameters of the methods and illustrated by many current practical applications including chiral analyses of drugs, their (bio)degradation products and biomarkers in pharmaceutical and biological matrices. The author wishes the readers many inspirations in the creation of new innovative approaches in the field of advanced chiral electrophoresis techniques with the aim to overcome capabilities of the current analytical techniques.

HPLC Methods for Pharmaceutical Analysis

HPLC Methods for Pharmaceutical Analysis
A Book

by George Lunn,Norman R. Schmuff

  • Publisher : Wiley-Interscience
  • Release : 1997
  • Pages : 2327
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Full text included in Knovel Library within the subject area of Chemistry and Chemical Engineering.

Handbook of Capillary and Microchip Electrophoresis and Associated Microtechniques, Third Edition

Handbook of Capillary and Microchip Electrophoresis and Associated Microtechniques, Third Edition
A Book

by James P. Landers

  • Publisher : CRC Press
  • Release : 2007-12-18
  • Pages : 1592
  • ISBN : 9781420004953
  • Language : En, Es, Fr & De
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Although capillary electrophoresis (CE) technology has evolved quickly from the research laboratory into practical application in numerous fields, many scientists still debate its merits. While the body of international CE literature continues to expand dramatically, experts still question whether it has provided the speed, resolving power, peak capacity, sensitivity, robustness, and cost-reduction promised by its pioneers. Responding to these criticisms, this third edition brings together cutting-edge researchers to demonstrate the utility of CE across a broad spectrum of disciplines including— Forensic science Medical diagnostics Pharmaceutical science Genetic analysis Biotechnology Fluid mechanics Environmental science Biomedical research Nanotechnology Proteomics Detailed Analysis of New Methodologies and Applications Eagerly awaited by researchers and technicians who transformed the first two editions into bestsellers, this latest volume once again delivers. Emphasizing microseparations and microfluidics, the Handbook of Capillary and Microchip Electrophoresis, Third Edition features new chapters describing the use of microchip electrophoresis and associated microtechniques, with a focus on the extraordinary breadth of work undertaken to expand CE methodologies in recent years. Aided by contributions from leading international experts, this text remains a seminal reference for numerous chemistry, biology, and engineering fields.

Capillary Electrophoresis - Mass Spectrometry (CE-MS)

Capillary Electrophoresis - Mass Spectrometry (CE-MS)
Principles and Applications

by Gerhardus de Jong

  • Publisher : John Wiley & Sons
  • Release : 2016-09-13
  • Pages : 368
  • ISBN : 3527339248
  • Language : En, Es, Fr & De
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This monograph offers the reader a complete overview on both principles and applications of CE-MS. Starting with an introductory chapter on detection in CE, also related and more specialized techniques such as electrophoretic and chromatographic preconcentration are discussed. A special emphasis is put on CE-MS interfaces, which are described in detail. In a separate chapter, attention is paid to sheath-liquid interfacing. The developments and possibilities of microchip CE-MS are also described. Applications to all relevant areas are discussed in distinct chapters, each written by experts in the respective fields. Besides applications in pharmaceutical analysis and bioanalysis, recent implementations in food science, forensic analysis, analysis of intact proteins, metabolomics and proteomics are highlighted. MS is a perfectly appropriate detection system for CE, as efficient separation is coupled to sensitive and selection detection. Moreover, MS can provide structure information on the separated compounds. CE-MS has now been developed into a strong hyphenated system complementary to LC-MS. This monograph is an unique source of knowledge for everyone dealing with and interested in CE-MS.

Handbook of Pharmaceutical Analysis

Handbook of Pharmaceutical Analysis
A Book

by Lena Ohannesian,Anthony Streeter

  • Publisher : CRC Press
  • Release : 2001-11-09
  • Pages : 608
  • ISBN : 9780824741945
  • Language : En, Es, Fr & De
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Exploring the analysis of pharmaceuticals, including polymorphic forms, this book discusses regulatory requirements in pharmaceutical product development and pharmaceutical testing. It covers methods of drug separation and procedures such as capillary electrophoresis for chromatographic separation of molecules. Additional topics include drug formulation analysis using vibrational and magnetic resonance spectroscopy and identification of drug metabolites and decomposition products using such techniques as mass spectrometry. The book provides more than 300 tables, equations, drawings, and photographs, and convenient, easy-to-use indices, facilitating quick access to each topic.

The British National Bibliography

The British National Bibliography
A Book

by Arthur James Wells

  • Publisher : Unknown Publisher
  • Release : 2000
  • Pages : 329
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Capillary Electrophoresis Guidebook

Capillary Electrophoresis Guidebook
Principles, Operation, and Applications

by Kevin D. Altria

  • Publisher : Springer Science & Business Media
  • Release : 1996
  • Pages : 349
  • ISBN : 1592595391
  • Language : En, Es, Fr & De
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Capillary Electrophoresis Guidebook offers both newcomers and experienced research workers hands-on guidance to performing capillary electrophoresis. It provides sufficient practical advice to permit you to develop and optimize your own separations, along with extensive troubleshooting sections to overcome practical difficulties. The book contains operating instructions for standard commercially available instruments and includes guidelines for activities such as changing capillaries, method development, quantitative procedures, optimizing sensitivity, and the validation of methods. Review chapters written by leading experts discuss micellar electrokinetic capillary chromatography, capillary gel electrophoresis, advanced sampling techniques, and electrochromatography. Important application areas such as the analysis of proteins, peptides, amino acids, pharmaceuticals, chiral compounds, and nucleic acids are also treated.

Multivariate Methods in Chromatography

Multivariate Methods in Chromatography
A Practical Guide

by Tibor Cserhati

  • Publisher : John Wiley & Sons Incorporated
  • Release : 2008-08-25
  • Pages : 335
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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A comprehensive, compilation and evaluation of the newest results in the field of enumerate evaluation of chromatographic data Aimed at the practicing professional, researchers and advanced students working in this area Special emphasis on practical applications While the principles of chromatography and multivariate mathematical-statistical methods are discussed separately, the book focuses on their interconnection. Written by a chromatographer for chromatographers

Pharmaceutical Analysis

Pharmaceutical Analysis
A Textbook for Pharmacy Students and Pharmaceutical Chemists

by David G. Watson

  • Publisher : Churchill Livingstone
  • Release : 2005
  • Pages : 382
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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This introductory text highlights the most important aspects of a wide range of techniques used in the control of the quality of pharmaceuticals. Written with the needs of the student in mind, this clear, practical guide includes self-testing sections with arithmetical examples and tests to help students brush up on their arithmetical skills in an applied context. Covers all of the most important analysis techniques in one book. Concentrates on the most important points with just the right level of detail. Summarizes the relevant theory but avoids becoming too esoteric. Features chapter summaries, key points and self-assessment boxes. Includes arithmetical calculations of results in the self-assessment exercises. Additional section on basic calculations in pharmaceutical analysis More detail on the capillary electrophoresis of proteins A discussion of some of the new types of HPLC column and on solvent selectivity in HPLC Additional material inserted on the control of the quality of analytical methods, mass spectrometry and high pressure liquid chromatography Additional self-assessment exercises

NMR Spectroscopy in Pharmaceutical Analysis

NMR Spectroscopy in Pharmaceutical Analysis
A Book

by Iwona Wawer,Bernd Diehl

  • Publisher : Elsevier
  • Release : 2017-07-07
  • Pages : 528
  • ISBN : 008095152X
  • Language : En, Es, Fr & De
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For almost a decade, quantitative NMR spectroscopy (qNMR) has been established as valuable tool in drug analysis. In all disciplines, i. e. drug identification, impurity profiling and assay, qNMR can be utilized. Separation techniques such as high performance liquid chromatography, gas chromatography, super fluid chromatography and capillary electrophoresis techniques, govern the purity evaluation of drugs. However, these techniques are not always able to solve the analytical problems often resulting in insufficient methods. Nevertheless such methods find their way into international pharmacopoeias. Thus, the aim of the book is to describe the possibilities of qNMR in pharmaceutical analysis. Beside the introduction to the physical fundamentals and techniques the principles of the application in drug analysis are described: quality evaluation of drugs, polymer characterization, natural products and corresponding reference compounds, metabolism, and solid phase NMR spectroscopy for the characterization drug substances, e.g. the water content, polymorphism, and drug formulations, e.g. tablets, powders. This part is accompanied by more special chapters dealing with representative examples. They give more detailed information by means of concrete examples. Combines theory, techniques, and concrete applications—all of which closely resemble the laboratory experience Considers international pharmacopoeias, addressing the concern for licensing Features the work of academics and researchers, appealing to a broad readership