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Solid-Phase Extraction

Solid-Phase Extraction
Principles, Techniques, and Applications

by Nigel J.K. Simpson

  • Publisher : CRC Press
  • Release : 2000-03-15
  • Pages : 528
  • ISBN : 9781420056242
  • Language : En, Es, Fr & De
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Demonstrating the relationship of the basic theory of solid-phase extraction (SPE) to chromatography, this comprehensive reference illustrates how SPE techniques significantly contribute to the preparation of samples for a wide variety of analytical techniques. It provides step-by-step details on the applications of SPE to environmental matrices, broad-spectrum drug screening, veterinary drug abuse, pharmaceutical drug development, biological samples, and high-throughput screening. Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.

Analytical Solid-Phase Extraction

Analytical Solid-Phase Extraction
A Book

by James S. Fritz,James Sherwood Fritz

  • Publisher : Wiley-VCH
  • Release : 1999-06-25
  • Pages : 209
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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New trends in solid-phase extraction for analytical use--a practical introduction. Owing to its low cost, ease of use, and nonpolluting means of preparing samples for analysis, solid-phase extraction (SPE) is fast overtaking traditional liquid--liquid methods in clinical, pharmaceutical, agricultural, and industrial applications. This book describes what analytical scientists and technicians need to know about this emerging procedure: how it works, how to choose from available techniques, how to utilize it effectively in the laboratory. Along with the historical perspective and fundamental principles, this practical book reviews the latest literature on solid-phase materials, equipment, and applications--including EPA-endorsed techniques. Special features include: * Coverage of separation and uptake methods. * Promising developments in the use of membrane disks. * The advantages of using polymeric resins over silica materials. * Mechanism and use of ion-exchange materials for SPE. * A remarkably complete chapter on the extraction of metal ions. * Groundbreaking research in the miniaturized SPE technique. Readers seeking additional information on SPE procedures may wish to consult: SOLID-PHASE EXTRACTION, Principles and Practice, E. M. Thurman and M. S. Mills 1998 (0-471-61422-X) 384 pp. SOLID-PHASE MICROEXTRACTION Theory and Practice Janusz Pawliszyn 1997 (0-471-19034-9) 264 pp.

Solid-Phase Extraction

Solid-Phase Extraction
A Book

by Colin F. Poole

  • Publisher : Elsevier
  • Release : 2019-09-12
  • Pages : 740
  • ISBN : 0128169079
  • Language : En, Es, Fr & De
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Solid Phase Extraction thoroughly presents both new and historic techniques for dealing with solid phase extraction. It provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample. In addition, the book showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including solid-phase Microextraction, molecularly imprinted polymers, magnetic nanoparticles, and more. Written by recognized experts in their respective fields, this one-stop reference is ideal for those who need to know which technique to choose for solid phase extraction. Used in conjunction with a similar release, Liquid Phase Extraction, this book allows users to master this crucial aspect of sample preparation. Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice Includes extensive referencing that facilitates the identification of key information Aimed at both entry-level scientists and those who want to explore new techniques and methods

Solid-Phase Extraction

Solid-Phase Extraction
Principles and Practice

by E. Michael Thurman,M. S. Mills,M. S.. Mills

  • Publisher : Wiley-Interscience
  • Release : 1998-03-16
  • Pages : 344
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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The final section of the book discusses the latest SPE technology, with detailed coverage of the automation process, solid-phase extraction disks, and innovations such as solid-phase microextraction and small-volume solid-phase extraction. Suggested reading and references are included throughout, providing a useful spring-board for further research and study.

Forensic and Clinical Applications of Solid Phase Extraction

Forensic and Clinical Applications of Solid Phase Extraction
A Book

by Michael J. Telepchak

  • Publisher : Springer Science & Business Media
  • Release : 2004-04-28
  • Pages : 370
  • ISBN : 1592592929
  • Language : En, Es, Fr & De
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This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.

Solid-Phase Extraction

Solid-Phase Extraction
Procedure, Applications and Effects

by Ben Benson

  • Publisher : Nova Science Publishers
  • Release : 2018
  • Pages : 153
  • ISBN : 9781536145823
  • Language : En, Es, Fr & De
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Conventional sample preparation techniques like solid phase extraction and liquid-liquid extraction prove to be tedious, time-consuming and oftentimes cumbersome. As a result, new sample techniques have been developed based on the two methods to optimize solvent consumption, miniaturize extraction and decrease environmental impact. In Solid-Phase Extraction: Procedure, Applications and Effects, the authors explore the recent developments and applications of solid phase microextraction techniques used in the preconcentration of personal care products.Following this, this collection addresses the use of chemical compounds for agriculture purposes which can cause the contamination of the environment. These contaminants can remain in the plant and soil or migrate from soil to water. As such, the authors suggest that the detection and quantification of pesticide residues in waters is of great concern.Membrane disk solid-phase extraction have been used to pretreat large-volume water samples because their large cross-section areas allow relatively high flow rates. Solid-phase extraction disks maintain their shape from the pretreatment process to the assaying step, making them useful for wet analyses as well as direct analyses.The closing chapter examines the development of the used solid-phase extraction sorbents since the introduction of the technique until today. Sample preparation always plays a key role in the chemical analysis of a variety of matrices and is the most time-consuming and complicated step of the entire analytical procedure.

Beginner's Guide to SPE

Beginner's Guide to SPE
Solid-Phase Extraction

by Waters Corporation

  • Publisher : Waters Corporation
  • Release : 2014-04-21
  • Pages : 212
  • ISBN : 9781467539203
  • Language : En, Es, Fr & De
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Through over 150 full color diagrams and straight forward text, readers will understand the power and usefulness of solid-phase extraction and how it helps solve sample preparation challenges. This 212 page book covers many topics including SPE device formats, sorbent considerations, mobile phase selection, and troubleshooting. A must read for anyone starting out in analytical chromatography as well as seasoned chemists looking to add solid-phase extraction to their skills set. Looking for something else? Learn a new technique or technology with the Waters Primers Series, view other titles available here: http://www.wiley.com/go/waters

Comparison of Cartridge and Membrane Solid-phase Extraction with Salting-out Solvent Extraction for Preconcentration of Nitroaromatic and Nitramine Explosives from Water

Comparison of Cartridge and Membrane Solid-phase Extraction with Salting-out Solvent Extraction for Preconcentration of Nitroaromatic and Nitramine Explosives from Water
A Book

by Anonim

  • Publisher : Unknown Publisher
  • Release : 1992
  • Pages : 31
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Solid Phase Extraction

Solid Phase Extraction
Principles and Applications

by Romeo-Iulian Olariu,Cecilia Arsene,Davide Vione,Nelu Grinberg

  • Publisher : CRC PressI Llc
  • Release : 2013-03-15
  • Pages : 400
  • ISBN : 9781439868324
  • Language : En, Es, Fr & De
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Solid Phase Microextraction

Solid Phase Microextraction
Theory and Practice

by Janusz Pawliszyn

  • Publisher : John Wiley & Sons
  • Release : 1997-04-21
  • Pages : 264
  • ISBN : 9780471190349
  • Language : En, Es, Fr & De
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Solid Phase Microextraction: Theory and Practice Janusz Pawliszyn Solid phase microextraction (SPME) is a recently proposed solvent-free sampling and sample preparation technique. SPME represents a quick, sensitive, and economical approach that can be adopted for field work and can be easily integrated with present analytical instrumentation into an automation process. Written by the inventor of the technique, Solid Phase Microextraction: Theory and Practice describes the theoretical and practical aspects of this new technology, which received an "R&D 100" Award in 1994 recognizing its invention as a major advancement in the analytical sciences. Solid Phase Microextraction: Theory and Practice, the first book on SPME, offers the reader: * An overview of SPME technique, theory, method development, and applications; * Experiments for beginners; * A summary of the practical applications of SPME in environmental, food, pharmaceutical, and forensic settings; * Material suitable for SPME courses or self-guided study.

Liquid-Phase Extraction

Liquid-Phase Extraction
A Book

by Colin F. Poole

  • Publisher : Elsevier
  • Release : 2019-08-29
  • Pages : 816
  • ISBN : 0128169125
  • Language : En, Es, Fr & De
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Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice Includes extensive referencing that facilitates the identification of key information Aimed at both entry-level scientists and those who want to explore new techniques and methods

Handbook of Solid Phase Microextraction

Handbook of Solid Phase Microextraction
A Book

by Janusz Pawliszyn

  • Publisher : Elsevier
  • Release : 2011-11-29
  • Pages : 496
  • ISBN : 0123914493
  • Language : En, Es, Fr & De
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The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner

Solid Phase Extraction in Sample Preparation

Solid Phase Extraction in Sample Preparation
An Applications Bibliography

by DIANE Publishing Company

  • Publisher : DIANE Publishing
  • Release : 1994-10
  • Pages : 48
  • ISBN : 9780788113444
  • Language : En, Es, Fr & De
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Designed to assist with specific extraction requirements. Contains over a thousand references to the use of Solid Phase Extraction in sample preparation, including method sheets, peer-reviewed articles, and surveys. Includes: analyte by compound, analyte by class, and reference table.

Evaluation of Sample Extract Cleanup Using Solid-phase Extraction Cartridges

Evaluation of Sample Extract Cleanup Using Solid-phase Extraction Cartridges
A Book

by Viorica Lopez-Avila,Janet Benedicto,June Milanes

  • Publisher : Unknown Publisher
  • Release : 1989
  • Pages : 124
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Analytical Microextraction Techniques

Analytical Microextraction Techniques
A Book

by M. Valcárcel,S. Cárdenas,R. Lucena

  • Publisher : Bentham Science Publishers
  • Release : 2017-01-13
  • Pages : 425
  • ISBN : 1681083795
  • Language : En, Es, Fr & De
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Sample treatment has been the focus of intensive research in the last 20 years since it still remains a bottleneck in precise analytical procedures. The low concentration of the target analytes, the large amount of potential interfering agents and the incompatibility of the sample matrix with the instrumental techniques are the main reasons for these bottlenecks. In most of these methods, sample treatment is an unavoidable step and it has a clear influence on the quality (sensitivity, selectivity, and accuracy) of the final analytical results. While the usefulness of microextraction techniques has been established, their complete acceptance in analytical laboratories (including official methods of analysis) depends on their successful automation and integration with conventional analytical instrumentation. Analytical Microextraction Techniques presents comprehensive information about several analytical methods that are useful in the laboratory. These include: sorptive microextraction, solid and liquid phase microextraction, packed sorbent microextraction, miniaturized dispersive solid-phase extraction, thin film and nanoparticle based techniques, and membrane-based techniques. This is a vital reference on microextraction and sample preparation techniques for applied chemistry students, analytical chemists and laboratory technicians.

Comparison of three solid phase extraction methods for the separation of cholestane-3b, 5a, 6b-triol and 25-hydroxycholesterol from cholesterol in turkey meat and processed products for an ELISA immunoassay

Comparison of three solid phase extraction methods for the separation of cholestane-3b, 5a, 6b-triol and 25-hydroxycholesterol from cholesterol in turkey meat and processed products for an ELISA immunoassay
A Book

by Clark D. Linde

  • Publisher : Unknown Publisher
  • Release : 1997
  • Pages : 136
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Federal Register

Federal Register
A Book

by Anonim

  • Publisher : Unknown Publisher
  • Release : 2013-05
  • Pages : 329
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Methods of Analysis by the U.S. Geological Survey National Water Quality Laboratory

Methods of Analysis by the U.S. Geological Survey National Water Quality Laboratory
Determination of Wastewater Compounds by Polystyrene-divinylbenzene Solid-phase Extraction and Capillary-column Gas Chromatography/mass Spectrometry

by Anonim

  • Publisher : Unknown Publisher
  • Release : 2002
  • Pages : 37
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Applications of Solid Phase Microextraction

Applications of Solid Phase Microextraction
A Book

by Janusz Pawliszyn

  • Publisher : Royal Society of Chemistry
  • Release : 1999
  • Pages : 655
  • ISBN : 9780854045259
  • Language : En, Es, Fr & De
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Applications of Solid Phase Microextraction (SPME) describes the applications of this technique as a modern alternative to current sample preparation technology. In industry, practical uses of SPME can be found in environmental, food, pharmaceutical, clinical and forensic applications, all of which are described in this book. New technologies are presented throughout, including new coatings and interfaces for analytical instrumentation, automation and calibration processes.

Metal Organic Frameworks

Metal Organic Frameworks
Synthesis and Application

by Victoria Samanidou,Eleni Deliyanni

  • Publisher : MDPI
  • Release : 2020-03-27
  • Pages : 198
  • ISBN : 303928486X
  • Language : En, Es, Fr & De
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Metal–organic frameworks are among the most promising novel materials. The concept of MOFs was first introduced in 1990. They were actually initially used in catalysis, gas separation, membranes, electrochemical sensors. Later on, they were introduced as SPE sorbents for PAHs (Polycyclic Aromatic Hydrocarbons) in environmental water samples, then the range expanded to the field of analytical chemistry, both in chromatographic separation and sample preparation, with great success in, e.g., SPE and SPME (Solid Phase Mico-extraction). Since then, the number of analytical applications implementing MOFs as sorbents in sorptive sample preparation approaches is increasing. Τhis is reinforced by the fact that, at least theoretically, an infinite number of structures can be designed and synthesized, thus making tuneability one of the most unique characteristics of MOF materials. Moreover, they have been designed in various shapes, such as columns, fibers, and films, so that they can meet more analytical challenges with improved analytical features.Their exceptional properties attracted the interest of analytical chemists who have taken advantage of the unique structures and properties and have already introduced them in several sample pretreatment techniques, such as solid phase extraction, dispersive SPE, magnetic solid phase extraction, solid phase microextraction, stir bar sorptive extraction, etc.