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Thermal Analysis in Practice

Thermal Analysis in Practice
Fundamental Aspects

by Matthias Wagner

  • Publisher : Unknown Publisher
  • Release : 2017-12
  • Pages : 352
  • ISBN : 9781569906439
  • Language : En, Es, Fr & De
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Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.

Thermal Analysis in Practice

Thermal Analysis in Practice
Collected Applications

by Matthias Wagner (kemik.)

  • Publisher : Unknown Publisher
  • Release : 2013
  • Pages : 327
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Thermal Analysis in Practice

Thermal Analysis in Practice
Fundamental Aspects

by Matthias Wagner

  • Publisher : Carl Hanser Verlag GmbH Co KG
  • Release : 2017-12-11
  • Pages : 350
  • ISBN : 1569906440
  • Language : En, Es, Fr & De
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Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.

Thermal Analysis in Practice

Thermal Analysis in Practice
Fundamental Aspects

by Matthias Wagner

  • Publisher : Unknown Publisher
  • Release : 2018
  • Pages : 352
  • ISBN : 9781523120222
  • Language : En, Es, Fr & De
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"Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis."--

Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Principles and Practice

by Michael E. Brown

  • Publisher : Elsevier
  • Release : 1998-09-07
  • Pages : 722
  • ISBN : 9780080539591
  • Language : En, Es, Fr & De
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Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.

Thermal Analysis of Plastics

Thermal Analysis of Plastics
Theory and Practice

by Gottfried W. Ehrenstein,Gabriela Riedel,Pia Trawiel

  • Publisher : Carl Hanser Verlag GmbH Co KG
  • Release : 2012-11-12
  • Pages : 400
  • ISBN : 3446434143
  • Language : En, Es, Fr & De
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Thermal analysis has proven to be one of the most important and meaningful test methods in the plastics industry and in testing laboratories. Although thermal analysis is used for fundamental studies related to materials science of polymers, its power lies in understanding this behavior during manufacturing processes. This understanding aids in process optimization, reduction of manufacturing cycle times, failure analysis as well as overall improvement of the material properties of the finished product, to name a few. In this book, the different test methods and their variations are described in detail, emphasizing the principles and their application in practice. Using practical examples, different approaches to problem solving are presented with a focus on the interpretation of the experimental results. Thermal analysis provides information on important properties of plastic materials, such as nucleation, crystallization, degree of crystallinity, recrystallization, melting and solidification, glass transition, curing and postcuring, thermal stability, thermal expansion, relaxation of orientation and internal stresses, pvT-data, and others. This book is a must for everybody involved in material and product development, testing, processing, quality assurance, or failure analysis in industry and laboratories. Contents: - Differential Scanning Calorimetry (DSC) - Oxidative Induction Time/Temperature (OIT) - Thermogravimetry (TG) - Thermo-Mechanical Analysis (TMA) - pvT-Measurements - Dynamic-Mechanical Analysis (DMA) - Micro-Thermal Analysis - Brief Characterization of Key Polymers

Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Principles and Practice

by Patrick Kent Gallagher,Michael E. Brown,Richard B. Kemp

  • Publisher : Elsevier Science Limited
  • Release : 1998
  • Pages : 722
  • ISBN : 9780444820853
  • Language : En, Es, Fr & De
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As a new field of interdisciplinary macromolecular science and engineering, polymeric materials will have a profound presence in 21st century chemical, pharmaceutical, biomedical, manufacturing, infrastructure, electronic, optical and information technologies. The origin of this field derived from an area of polymer science and engineering encompassing plastic technologies. The field is rapidly expanding to incorporate new interdisciplinary research areas such as biomaterials, macromolecular biology, novel macromolecular structures, environmental macromolecular science and engineering, innovative and nano-fabrications of products, and is translating discoveries into technologies.

Thermal Analysis of Materials

Thermal Analysis of Materials
A Book

by Robert Speyer

  • Publisher : CRC Press
  • Release : 1993-09-16
  • Pages : 298
  • ISBN : 1482277425
  • Language : En, Es, Fr & De
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Discussing the design and optimum use of thermal analysis instrumentation for materials' property measurement, this work details how the instruments work, what they measure, potential pitfalls and the fitting of experimental results to theoretical models. It presents a tutorial on writing computer programs for data manipulation, advanced thermoanalytical methods and case studies.

Recommended Practice for Thermal Analysis of Steel

Recommended Practice for Thermal Analysis of Steel
A Book

by Anonim

  • Publisher : Unknown Publisher
  • Release : 1936
  • Pages : 4
  • ISBN : 9876543210XXX
  • Language : En, Es, Fr & De
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Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Recent Advances, Techniques and Applications

by Anonim

  • Publisher : Elsevier
  • Release : 2011-09-22
  • Pages : 780
  • ISBN : 9780080556314
  • Language : En, Es, Fr & De
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This is Volume 5 of a Handbook that has been well-received by the thermal analysis and calorimetry community. All chapters in all five volumes are written by international experts in the subject. The fifth volume covers recent advances in techniques and applications that complement the earlier volumes. The chapters refer wherever possible to earlier volumes, but each is complete in itself. The latest recommendations on Nomenclature are also included. Amongst the important new techniques that are covered are micro-thermal analysis, pulsed thermal analysis, fast-scanning calorimetery and the use of quartz-crystal microbalances. There are detailed reviews of heating - stage spectroscopy, the range of electrical techniques available, applications in rheology, catalysis and the study of nanoparticles. The development and application of isoconversional methods of kinetic analysis are described and there are comprehensive chapters on the many facets of thermochemistry and of measuring thermophysical properties. Applications to inorganic and coordination chemistry are reviewed, as are the latest applications in medical and dental sciences, including the importance of polymorphism. The volume concludes with a review of the use and importance of thermal analysis and calorimetry in quality control. * Updates and complements previous volumes * Internationally recognized experts as authors * Each chapter complete in itself

Modulated Temperature Differential Scanning Calorimetry

Modulated Temperature Differential Scanning Calorimetry
Theoretical and Practical Applications in Polymer Characterisation

by Mike Reading,Douglas J. Hourston

  • Publisher : Springer Science & Business Media
  • Release : 2006-02-22
  • Pages : 328
  • ISBN : 9781402037498
  • Language : En, Es, Fr & De
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MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Recent Advances, Techniques and Applications

by Anonim

  • Publisher : Elsevier
  • Release : 2018-03-12
  • Pages : 860
  • ISBN : 0444640630
  • Language : En, Es, Fr & De
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Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications

Thermal Analysis of Plastics

Thermal Analysis of Plastics
Theory and Practice

by G. W. Ehrenstein,Gabriela Riedel,Pia Trawiel

  • Publisher : Hanser Verlag
  • Release : 2004
  • Pages : 368
  • ISBN : 9781569903629
  • Language : En, Es, Fr & De
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Thermal analysis has proven to be one of the most important and meaningful test methods in the plastics industry and in testing laboratories. Although thermal analysis is used for fundamental studies related to materials science of polymers, its power lies in understanding this behavior during manufacturing processes. This understanding aids in process optimization, reduction of manufacturing cycle times, failure analysis as well as overall improvement of the material properties of the finished product, to name a few. In this book, the different test methods and their variations are described in detail, emphasizing the principles and their application in practice. Using practical examples, different approaches to problem solving are presented with a focus on the interpretation of the experimental results. Thermal analysis provides information on important properties of plastic materials, such as nucleation, crystallization, degree of crystallinity, recrystallization, melting and solidification, glass transition, curing and postcuring, thermal stability, thermal expansion, relaxation of orientation and internal stresses, pvT-data, and others.

Dynamic Mechanical Analysis

Dynamic Mechanical Analysis
A Book

by Kevin P. Menard,Noah Menard

  • Publisher : CRC Press
  • Release : 2020-05-04
  • Pages : 260
  • ISBN : 0429529597
  • Language : En, Es, Fr & De
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Dynamic Mechanical Analysis (DMA) is a powerful technique for understanding the viscoelastic properties of materials. It has become a powerful tool for chemists, polymer and material scientists, and engineers. Despite this, it often remains underutilized in the modern laboratory. Because of its high sensitivity to the presence of the glass transition, many users limit it to detecting glass transitions that can’t be seen by differential scanning calorimetry (DSC). This book presents a practical and straightforward approach to understanding how DMA works and what it measures. Starting with the concepts of stress and strain, the text takes the reader through stress–strain, creep, and thermomechanical analysis. DMA is discussed as both the instrument and fixtures as well as the techniques for measuring both thermoplastic and thermosetting behavior. This edition offers expanded chapters on these areas as well as frequency scanning and other application areas. To help the reader grasp the material, study questions have also been added. Endnotes have been expanded and updated. Features Reflects the latest DMA research and technical advances Includes case studies to demonstrate the use of DMA over a range of industrial problems Includes numerous references to help those with limited materials engineering background Demonstrates the power of DMA as a laboratory tool for analysis and testing

Thermal Analysis of Polymers

Thermal Analysis of Polymers
Fundamentals and Applications

by Joseph D. Menczel,R. Bruce Prime

  • Publisher : John Wiley & Sons
  • Release : 2014-07-09
  • Pages : 696
  • ISBN : 1118995996
  • Language : En, Es, Fr & De
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Presents a solid introduction to thermal analysis, methods,instrumentation, calibration, and application along with thenecessary theoretical background. Useful to chemists, physicists, materials scientists, andengineers who are new to thermal analysis techniques, and toexisting users of thermal analysis who wish expand their experienceto new techniques and applications Topics covered include Differential Scanning Calorimetry andDifferential Thermal Analysis (DSC/DTA), Thermogravimetry,Thermomechanical Analysis and Dilatometry, Dynamic MechanicalAnalysis, Micro-Thermal Analysis, Hot Stage Microscopy, andInstrumentation. Written by experts in the various areas of thermalanalysis Relevant and detailed experiments and examples follow eachchapter.

Handbook of Thermal Analysis of Construction Materials

Handbook of Thermal Analysis of Construction Materials
A Book

by V.S. Ramachandran,Ralph M. Paroli,James J. Beaudoin,Ana H. Delgado

  • Publisher : William Andrew
  • Release : 2002-10-28
  • Pages : 702
  • ISBN : 0815517750
  • Language : En, Es, Fr & De
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This comprehensive book containing essential information on the applicability of thermal analysis techniques to evaluate inorganic and organic materials in construction technology should serve as a useful reference for the scientist, engineer, construction technologist, architect, manufacturer, and user of construction materials, standard-writing bodies, and analytical chemists. The material scientists at the National Research Council of Canada have established one of the best thermal analysis laboratories in the world. Various types of thermal analysis techniques have been applied successfully to the investigation of inorganic and organic construction materials. These studies have provided important information on the characterization of raw as well as finished materials, quality control, quantitative estimation, interrelationships between physical, chemical, mechanical, and durability characteristics. Information on the application of thermal analysis to construction materials is dispersed in literature and hence the IRC scientists embarked on producing a handbook, the first of its kind, incorporating the latest knowledge available in this field of activity. Almost all important construction materials have been included.

Principles and Applications of Thermal Analysis

Principles and Applications of Thermal Analysis
A Book

by Paul Gabbott

  • Publisher : John Wiley & Sons
  • Release : 2008-04-30
  • Pages : 480
  • ISBN : 0470698128
  • Language : En, Es, Fr & De
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Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Thermal Stress Analysis of Composite Beams, Plates and Shells

Thermal Stress Analysis of Composite Beams, Plates and Shells
Computational Modelling and Applications

by Erasmo Carrera,Fiorenzo A. Fazzolari,Maria Cinefra

  • Publisher : Academic Press
  • Release : 2016-11-25
  • Pages : 440
  • ISBN : 0124200931
  • Language : En, Es, Fr & De
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Thermal Stress Analysis of Composite Beams, Plates and Shells: Computational Modelling and Applications presents classic and advanced thermal stress topics in a cutting-edge review of this critical area, tackling subjects that have little coverage in existing resources. It includes discussions of complex problems, such as multi-layered cases using modern advanced computational and vibrational methods. Authors Carrera and Fazzolari begin with a review of the fundamentals of thermoelasticity and thermal stress analysis relating to advanced structures and the basic mechanics of beams, plates, and shells, making the book a self-contained reference. More challenging topics are then addressed, including anisotropic thermal stress structures, static and dynamic responses of coupled and uncoupled thermoelastic problems, thermal buckling, and post-buckling behavior of thermally loaded structures, and thermal effects on panel flutter phenomena, amongst others. Provides an overview of critical thermal stress theory and its relation to beams, plates, and shells, from classical concepts to the latest advanced theories Appeals to those studying thermoelasticity, thermoelastics, stress analysis, multilayered structures, computational methods, buckling, static response, and dynamic response Includes the authors' unified formulation (UF) theory, along with cutting-edge topics that receive little coverage in other references Covers metallic and composite structures, including a complete analysis and sample problems of layered structures, considering both mesh and meshless methods Presents a valuable resource for those working on thermal stress problems in mechanical, civil, and aerospace engineering settings

Adaptive Thermal Comfort: Principles and Practice

Adaptive Thermal Comfort: Principles and Practice
A Book

by Fergus Nicol,Michael Humphreys,Susan Roaf

  • Publisher : Routledge
  • Release : 2012-03-15
  • Pages : 208
  • ISBN : 1136336478
  • Language : En, Es, Fr & De
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The fundamental function of buildings is to provide safe and healthy shelter. For the fortunate they also provide comfort and delight. In the twentieth century comfort became a 'product' produced by machines and run on cheap energy. In a world where fossil fuels are becoming ever scarcer and more expensive, and the climate more extreme, the challenge of designing comfortable buildings today requires a new approach. This timely book is the first in a trilogy from leaders in the field which will provide just that. It explains, in a clear and comprehensible manner, how we stay comfortable by using our bodies, minds, buildings and their systems to adapt to indoor and outdoor conditions which change with the weather and the climate. The book is in two sections. The first introduces the principles on which the theory of adaptive thermal comfort is based. The second explains how to use field studies to measure thermal comfort in practice and to analyze the data gathered. Architects have gradually passed responsibility for building performance to service engineers who are largely trained to see comfort as the ‘product’, designed using simplistic comfort models. The result has contributed to a shift to buildings that use ever more energy. A growing international consensus now calls for low-energy buildings. This means designers must first produce robust, passive structures that provide occupants with many opportunities to make changes to suit their environmental needs. Ventilation using free, natural energy should be preferred and mechanical conditioning only used when the climate demands it. This book outlines the theory of adaptive thermal comfort that is essential to understand and inform such building designs. This book should be required reading for all students, teachers and practitioners of architecture, building engineering and management – for all who have a role in producing, and occupying, twenty-first century adaptive, low-carbon, comfortable buildings.

Thermal Analysis with SolidWorks Simulation 2013

Thermal Analysis with SolidWorks Simulation 2013
A Book

by Paul M. Kurowski

  • Publisher : SDC Publications
  • Release : 2013
  • Pages : 191
  • ISBN : 1585037850
  • Language : En, Es, Fr & De
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Thermal Analysis with SolidWorks Simulation 2013 goes beyond the standard software manual. It concurrently introduces the reader to thermal analysis and its implementation in SolidWorks Simulation using hands-on exercises. A number of projects are presented to illustrate thermal analysis and related topics. Each chapter is designed to build on the skills and understanding gained from previous exercises. Thermal Analysis with SolidWorks Simulation 2013 is designed for users who are already familiar with basics of Finite Element Analysis (FEA) using SolidWorks Simulation or who have completed the book Engineering Analysis with SolidWorks Simulation 2013. Thermal Analysis with SolidWorks Simulation 2013 builds on these topics in the area of thermal analysis. Some understanding of FEA and SolidWorks Simulation is assumed.